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Pulse and Fourier Transform Nmr Introduction to Theory and Methods cover
  • ISBN: 9780122496509
  • ISBN10: 0122496507

Pulse and Fourier Transform Nmr Introduction to Theory and Methods

by Thomas Clark Farrar

  • List Price: $72.95
  • Binding: Hardcover
  • Publisher: Lightning Source Inc
  • Publish date: 06/01/1971
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Preface Acknowledgments Symbols and Abbreviations 1. Basic Concepts in NMR 1.1. Relaxation and Nuclear Magnetic Energy Levels 1.2. Some Basic Properties of Vectors 1.3. Nuclear Precession 1.4. The Bloch Equations 1.5. The Rotating Frame of Reference 1.6. Magnetization in the Rotating Frame 1.7. Fourier Analysis and Fourier Transformation 2. Free Induction and Spin Echoes 2.1. Free Induction Decay 2.2. Measurement of T1 2.3. Measurement of T2 by the Spin-Echo Method 2.4. The Carr-Purcell Technique 2.5. The Meiboom-Gill Method 2.6. Fourier Transform Methods 2.7. Weak Pulses and Selective Relaxation Measurements 2.8. Summary of Basic Pulse Methods 3. Instrumentation 3.1. The Pulsed NMR Spectrometer 3.2. The NMR Sample Probe 3.3. The rf Gate, Pulse Programmer, and rf Transmitter 3.4. The Amplification and Detection System 3.5. Systematic Errors in Pulsed NMR Instruments 4. Relaxation Mechanisms 4.1. Frequency Distribution of Molecular Motions 4.2. Spin-Lattice Interactions 4.3. Dipole-Dipole Relaxation 4.4. Quadrupole Relaxation 4.5. Relaxation via Chemical Shift Anisotropy 4.6. Scalar Relaxation 4.7. Spin-Rotation Relaxation 4.8. Summary of Relaxation Mechanisms 5. Fourier Transform NMR 5.1. Use of the FT Method in Multispin Systems 5.2. Instrumental Requirements 5.3. Computer Requirements 5.4. Effect of 1 on Signal/Noise Improvement 5.5. Multiple-Pulse Techniques 5.6. Transient Species; Measurement of Relaxation Times 5.7. Stochastic Excitation 6. Rotating Frame Experiments 6.1. Transient Nutations 6.2. Rotary Spin Echoes 6.3. Forced Transitory Precession; "Spin Locking" 6.4. Waugh Pulse Sequences 7. Selected Applications 7.1. Molecular Diffusion 7.2. Chemical Rate Processes 7.3. Molecular Dynamics References Subject Index
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